Name: ESRA-RAM-0001: Raman Spectroscopy of Cell 2026_DongMinKim_BrettHelms_ACS.Energy.Lett._6c00026
Creator: Dong-Min Kim
Published: 2026-08-12
License: https://spdx.org/licenses/CC-BY-4.0

Researcher

Dong-Min Kim

ORCID

0000-0003-0676-8208

PI(s)

Yan Yao; Mary C. Scott; Ying Chen; Brett A. Helms

Project

Thermoformable Electrolytes for Solid-State Sodium Metal Batteries Employing Organic Cathodes

Sample ID

2026_DongMinKim_BrettHelms_ACS.Energy.Lett._6c00026 ← click to see all uploads with this sample ID

Publication DOI

10.1021/acsenergylett.6c00026 ↗

Upload Date (CDT)

2026-08-12 22:27:58

Upload ID

58021d54-a2aa-42e2-8e14-7edce8d6be3d

How to Cite

1 — Cite the dataset paper

↗ View paper

2 — Cite the ESRA platform

Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform

CC BY 4.0 · Data shared under Creative Commons Attribution 4.0

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Notes

Raman fields

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Excitation Wavelength Nm *

Laser Power Mw

Exposure Time S

Num Accumulations

Wavenumber Min Cm1

Wavenumber Max Cm1

Materials studied

Shared by all 5 datasets on 2026_DongMinKim_BrettHelms_ACS.Energy.Lett._6c00026. Edits apply to every one.

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Storage LocationNERSC Community File System

Path

/global/cfs/cdirs/m4845/gsharing/yan-yao-mary-c-scott-ying-chen-brett-a-h/thermoformable-electrolytes-for-solid-st/2026-dongminkim-bretthelms-acsenergylett/Raman/raman/ESRA-RAM-0001/

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Linked Uploads

Other datasets with the same sample ID (2026_DongMinKim_BrettHelms_ACS.Energy.Lett._6c00026).

Type	Group	Date	Project	Link
XRD	Yan Yao; Mary C. Scott; Ying Chen; Brett A. Helms	2026-08-12 22:28	Thermoformable Electrolytes for Solid-State Sodium Metal Batteries Employing Organic Cathodes	same sample
NMR	Yan Yao; Mary C. Scott; Ying Chen; Brett A. Helms	2026-08-12 22:27	Thermoformable Electrolytes for Solid-State Sodium Metal Batteries Employing Organic Cathodes	same sample
EIS	Yan Yao; Mary C. Scott; Ying Chen; Brett A. Helms	2026-08-12 22:27	Thermoformable Electrolytes for Solid-State Sodium Metal Batteries Employing Organic Cathodes	same sample
Cycling	Yan Yao; Mary C. Scott; Ying Chen; Brett A. Helms	2026-08-12 22:27	Thermoformable Electrolytes for Solid-State Sodium Metal Batteries Employing Organic Cathodes	same sample

Materials Studied 5 materials

Material	Family	Role(s)	Ion
ORION electrolyte (zwitterionic sulfonate building unit + NaTFSI + ether ligand) · Thermoformable organo-ionic electrolyte Viscoelastic liquid above 110 C, solid at operating temperature; 3.4e-3 to 1.0 mS/cm Made in this work Formulation Vacuum dry — Dehydrate SBU and NaTFSI before use temperature: 60 °C SI p. 4, Preparation of ORION electrolyte Dry — Dry ether ligands G1/G2 over molecular sieves before use solvent: G1/G2 SI p. 4, Preparation of ORION electrolyte Ball mill — Ball-mill SBU with NaTFSI duration: 1 hequipment: Mini-mill Pulverisette 23composition ratio: SBU(SO3–) : NaTFSI = 1 : x, x = 0.5, 1.0, 2.0 duty cycle: 5 min relaxation in every 10 min SI p. 3, Preparation of ORION electrolyte Add — Add ether ligand G1 or G2 composition ratio: SBU(SO3–) : NaTFSI : G1/G2 (–O–) = 1 : 1 : y/z; G1 y = 1.0-3.0, G2 z = 1.0-3.5 SI pp. 3-4, Preparation of ORION electrolyte Heat — Heat on a heating plate and stir with a spatula every 1 h for homogeneous mixing duration: 4 hequipment: heating platetemperature: 110 °C stir interval: 1 h SI p. 4, Preparation of ORION electrolyte	Zwitterionic organo-ionic coordination solid Polymer SE · as named	Electrolyte	Na
NaTFSI · Sodium bis(trifluoromethanesulfonyl)imide Purchased / commercial Solvionic Sample preparation Vacuum dry — Dehydrate before use temperature: 60 °C SI, Preparation of ORION electrolyte	Sodium imide salt Other · as named	Salt	Na
1,2-dimethoxyethane (G1) / 1-methoxy-2-(2-methoxyethoxy)ethane (G2) · Na+-coordinating ether ligand Tunes Na+ coordination number up to 2.5 Purchased / commercial Sigma Aldrich Sample preparation Dry — Dehydrate over molecular sieves before use equipment: molecular sieves SI, Preparation of ORION electrolyte	Ether / glyme Liquid	Solvent, Additive	Na
PTCDA (perylene-3,4,9,10-tetracarboxylic dianhydride) · Organic cathode Electrolyte-infiltrated porous organic cathode composite, cycled at 60 C Purchased / commercial Electrode fabrication Vacuum dry — Dry the PTCDA cathode before cell assembly duration: overnighttemperature: 60 °C SI, cathode preparation	Organic carbonyl / quinone Cathode	Cathode	Na
Na metal · Sodium metal anode Purchased / commercial Sigma Aldrich Sample preparation Cut — Trim the Na metal cubes SI, cell assembly Calender — Roll flat SI, cell assembly Punch — Punch to 10 mm disks thickness: 10 mm diameter disks SI, cell assembly	Alkali metal Anode	Anode	Na

Declared for sample 2026_DongMinKim_BrettHelms_ACS.Energy.Lett._6c00026 — shared by every dataset on this sample.

Experiment Metadata

Scan Type	Single point
Visibility	public
Laser Power Mw	6.0
Exposure Time S	5.0
Publication Doi	10.1021/acsenergylett.6c00026
Institution Code	ESRA
Num Accumulations	20.0
Wavenumber Max Cm1	1300.0
Wavenumber Min Cm1	500.0
Excitation Wavelength Nm	532.0

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