Name: ESRA-SEM-0036: Scanning Electron Microscopy of Cell NBH-2024-12-CRYO
Creator: Thomas Marchese
Published: 2026-09-25
License: https://spdx.org/licenses/CC-BY-4.0

Researcher

Thomas Marchese

ORCID

0000-0002-3668-5000

PI(s)

Ying Shirley Meng; Mary C. Scott

Project

Sodium expulsion from sodium closo-hydroborates under electron beam induced bias

Sample ID

NBH-2024-12-CRYO ← click to see all uploads with this sample ID

Publication DOI

10.1093/mam/ozag104 ↗

Notes

Beam-damage / dose experiment series recorded as TIFF image frames and .avi movies (frames combined into movies; large exposures split into several movie sequences). Condition defined by beam voltage, beam current and sample temperature (cryo, 79 K stage); geometry: top-down, 0° tilt. Condition folder(s): 3.2nA exp1; 3.2 exp 2; 3.2nA exp 3; 3.2nA exp4; 3.2nA exp5; 3.2nA exp 6. Six exposure folders (exp 1-6). Reference-still file names say '13.2nA' but the instrument header records 3.2 nA in every reference still; 3.2 nA used.

Upload Date (CDT)

2026-09-25 16:57:01

Upload ID

7cedccfa-f751-489f-8d6e-a8bbb5ce1f1e

How to Cite

1 — Cite the dataset paper

↗ View paper

2 — Cite the ESRA platform

Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform

CC BY 4.0 · Data shared under Creative Commons Attribution 4.0

You must log in to edit this record.

PI Name(s)

Project

Sample ID

Publication DOI

Notes

SEM fields

Fill any blank required field to clear the Incomplete flag.

Accelerating Voltage Kv *

Detector Mode *

Sample Preparation *

Instrument Model

Sample Transfer

Materials studied

Shared by all 28 datasets on NBH-2024-12-CRYO. Edits apply to every one.

No materials declared yet.

or press Ctrl S

Researcher name, ORCID and experiment type cannot be changed after upload.

Storage LocationNERSC Community File System

Path

/global/cfs/cdirs/m4845/gsharing/ying-shirley-meng-mary-c-scott/sodium-expulsion-from-sodium-closo-hydro/nbh-2024-12-cryo/3.2nA exp 6/sem/ESRA-SEM-0036/

Open in Globus File Manager →

Linked Uploads

Other datasets with the same sample ID (NBH-2024-12-CRYO).

Type	Group	Date	Project	Link
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:57	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:56	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:56	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:56	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:56	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:56	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:55	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:55	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample
SEM	Ying Shirley Meng; Mary C. Scott	2026-09-25 16:55	Sodium expulsion from sodium closo-hydroborates under electron beam induced bias	same sample

Materials Studied 2 materials

Material	Family	Role(s)	Ion
Na2B10H10 · NBH10 Purchased precursor (not made for this work); listed in the SI of Deysher et al., Nat. Energy 2024, https://doi.org/10.1038/s41560-024-01569-9. Purchased / commercial	Borohydride / complex hydride Inorganic SE	Electrolyte	Na
Na4(B10H10)(B12H12) · NBH Made following an earlier paper https://doi.org/10.1038/s41560-024-01569-9	Borohydride / complex hydride Inorganic SE	Electrolyte	Na

Declared for sample NBH-2024-12-CRYO — shared by every dataset on this sample.

Experiment Metadata

Spot Size	13.0
Image Size	3072x2048
Visibility	public
Beam Current	3.2
Recorded Data	TIFF image frames and .avi movies (frames combined into movie sequences)
Detector Mode	ETD secondary electron (SE), high vacuum
Publication Doi	10.1093/mam/ozag104
Sample Transfer	Inert (Ar) transfer from the glovebox using a Thermo Fisher Scientific (TFS) QuickConnect sample loader
Chamber Pressure	0.941-1.13
Source Folder(S)	cryo SEM dose exp Mixed NBH/3.2nA exp1; cryo SEM dose exp Mixed NBH/3.2 exp 2; cryo SEM dose exp Mixed NBH/3.2nA exp 3; cryo SEM dose exp Mixed NBH/3.2nA exp4; cryo SEM dose exp Mixed NBH/3.2nA exp5; cryo SEM dose exp Mixed NBH/3.2nA exp 6
Working Distance	8.24-8.25
Institution Code	ESRA
Instrument Model	Thermo Fisher Aquilos DualBeam (SEM/FIB), FEG source
Specimen Geometry	top-down
Reference Still(S)	cryo SEM dose exp Mixed NBH/3.2nA exp1/3.2nA exp1/pre 5kv to image 20kx 13.2nA_020.tif; cryo SEM dose exp Mixed NBH/3.2 exp 2/3.2 exp 2/pre 5kv to image 20kx 13.2nA_022.tif; cryo SEM dose exp Mixed NBH/3.2nA exp 3/3.2nA exp 3/post 5kv to image 20kx 13.2nA_024.tif; cryo SEM dose exp Mixed NBH/3.2nA exp4/3.2nA exp4/pre 5kv to image 20kx 13.2nA_026.tif; cryo SEM dose exp Mixed NBH/3.2nA exp5/3.2nA exp5/pre 5kv to image 20kx 13.2nA_029.tif; cryo SEM dose exp Mixed NBH/3.2nA exp 6/3.2nA exp 6/pre 5kv to image 20kx 13.2nA_.tif
Sample Temperature	cryo
Sample Preparation	Pelletized NBH powder prepared in an Ar glovebox; pellet fixed to the SEM stub with carbon tape
Detector Mode Source	TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 13.2nA_020.tif
Data Location (Local)	I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2nA exp1; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2 exp 2; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2nA exp 3; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2nA exp4; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2nA exp5; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\3.2nA exp 6
Accelerating Voltage Kv	5.0
Instrument Model Source	TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 13.2nA_020.tif
Stage Temperature (Header)	79.2
Dwell Time (Reference Still)	3.0
Experiment Folders In Record	6.0
Stage Tilt (Reference Still)	0.0
Accelerating Voltage Kv Source	TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 13.2nA_020.tif
Acquisition Date(S) (Reference Stills)	2024-12-12
Horizontal Field Width (Reference Still)	20.7

Uploaded Files 168 files · 865.4 MB

Versions 0 saved

A version freezes the description and the list of files at one moment, so a paper can say which one it used. The ESRA ID stays the same. Saved automatically when a dataset is made public, and by hand below.

No version saved yet.