Name: ESRA-CYC-0010: Galvanostatic Cycling (charge–discharge) of Cell 2025_DarenWu_KelseyHatzell_EES.Batteries_d5eb00097a
Creator: Daren Wu
Published: 2026-08-14
License: https://spdx.org/licenses/CC-BY-4.0

Researcher

Daren Wu

ORCID

0000-0002-5222-7288

PI(s)

Kelsey B. Hatzell

Project

Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries

Sample ID

2025_DarenWu_KelseyHatzell_EES.Batteries_d5eb00097a ← click to see all uploads with this sample ID

Publication DOI

10.1039/d5eb00097a ↗

Upload Date (CDT)

2026-08-14 15:06:30

Upload ID

a2c3a703-4546-42f0-a5e5-17f463cc85bd

How to Cite

1 — Cite the dataset paper

↗ View paper

2 — Cite the ESRA platform

Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform

CC BY 4.0 · Data shared under Creative Commons Attribution 4.0

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PI Name(s)

Project

Sample ID

Publication DOI

Notes

Cycling fields

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Cell Type

Cathode Material *

Anode Material *

Cell Geometry *

Cell Geometry Verbatim

Electrode Area Cm2 *

Active Mass Cathode Mg

Active Mass Anode Mg

Specific Capacity Mah G

Theoretical Capacity Mah

Temperature C

Electrolyte

Voltage Window Lower V

Voltage Window Upper V

Stack Pressure Mpa

Protocol Summary

Number Of Cycles

Materials studied

Shared by all 8 datasets on 2025_DarenWu_KelseyHatzell_EES.Batteries_d5eb00097a. Edits apply to every one.

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Storage LocationNERSC Community File System

Path

/global/cfs/cdirs/m4845/gsharing/kelsey-b-hatzell/chemo-mechanical-limitations-of-liquid-a/2025-darenwu-kelseyhatzell-eesbatteries/DW1_85A1_K cell/cycling/ESRA-CYC-0010/

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Linked Uploads

Other datasets with the same sample ID (2025_DarenWu_KelseyHatzell_EES.Batteries_d5eb00097a).

Type	Group	Date	Project	Link
XCT	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
EIS	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
EIS	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
Cycling	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
Cycling	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
Cycling	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample
Cycling	Kelsey B. Hatzell	2026-08-14 15:06	Chemo-mechanical limitations of liquid alloy anodes for sodium solid-state batteries	same sample

Materials Studied 2 materials

Material	Family	Role(s)	Ion
Na-K liquid alloy (NaK50, NaK65, NaK80) · Liquid NaK alloy anode Room-temperature liquid alkali-metal alloy; Na:K ratio varied	Alloy Anode	Anode	Na
Na3Zr2Si2PO12 · NASICON solid electrolyte Purchased / commercial MSE Supplies Material synthesis Press — Cold press the commercial NASICON powder pressure: 625 MPa Methods, Preparation of NASICON solid-state electrolyte Sinter — Sinter to a self-standing pellet duration: 12 hthickness: ~1500 umtemperature: 1230 °Cheating rate: 5 °C min-1 Methods, Preparation of NASICON solid-state electrolyte Sputter — Sputter 20 nm Sn onto the NaK-contacting NASICON surface equipment: VCR IBS/TM200S Ion Beam Sputterersubstrate: as-sintered NASICON pellet surfacethickness: 0.02 um Methods, Preparation of NASICON solid-state electrolyte Anneal — Anneal in a tube furnace to form the SnO2 coating duration: 3 hequipment: tube furnacetemperature: 900 °C Methods, Preparation of NASICON solid-state electrolyte	NASICON Inorganic SE	Electrolyte	Na

Declared for sample 2025_DarenWu_KelseyHatzell_EES.Batteries_d5eb00097a — shared by every dataset on this sample.

Experiment Metadata

Visibility	public
Electrolyte	Na₃Zr₂Si₂PO₁₂ (NASICON) with 20 nm SnO₂ coating
Anode Material	Na-K liquid alloy
Publication Doi	10.1039/d5eb00097a
Number Of Cycles	run until short-circuit; pulsed stripping: multiple pulses (varies per rest condition)
Cathode Material	Na metal
Institution Code	ESRA
Electrode Area Cm2	0.503
Voltage Window — Upper	3.0
Current / C-Rate / Protocol Summary	CCD: 0.05, 0.1, 0.2, 0.4 mA cm⁻² (Na stripping/plating); SGEIS: 0.05–1 mA cm⁻², step 0.01 mA cm⁻²; pulsed: 1 mA cm⁻², 1 s pulse + 0.1–10 s rest

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