Browse Data ESRA-SEM-0037 SEM Public
Thomas Marchese
0000-0002-3668-5000
Ying Shirley Meng; Mary C. Scott
Sodium expulsion from sodium closo-hydroborates under electron beam induced bias
NBH-2024-12-CRYO ← click to see all uploads with this sample ID
10.1093/mam/ozag104 ↗
Beam-damage / dose experiment series recorded as TIFF image frames and .avi movies (frames combined into movies; large exposures split into several movie sequences). Condition defined by beam voltage, beam current and sample temperature (cryo, 79 K stage); geometry: top-down, 0° tilt. Condition folder(s): 6.4nA exp1; 6.4 exp 2; 6.2 exp 3. Folder 'exp 3' is labelled 6.2 nA; the instrument header records 6.4 nA for all three reference stills; 6.4 nA used.
2026-09-25 16:57:03
ad2474f2-8690-49db-8208-9539115319f0
How to Cite
1 — Cite the dataset paper
↗ View paper
2 — Cite the ESRA platform
Galib, M. et al. (2026). ESRA: Energy Storage Research Assistant. Argonne National Laboratory. https://github.com/MusannaGalib/esra-platform
CC BY 4.0  ·  Data shared under Creative Commons Attribution 4.0

Storage LocationNERSC Community File System

/global/cfs/cdirs/m4845/gsharing/ying-shirley-meng-mary-c-scott/sodium-expulsion-from-sodium-closo-hydro/nbh-2024-12-cryo/6.4nA exp1/sem/ESRA-SEM-0037/
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Linked Uploads

Other datasets with the same sample ID (NBH-2024-12-CRYO).

Type Group Date Project Link
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:57 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:56 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:56 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:56 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:56 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:56 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:55 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:55 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample
SEM Ying Shirley Meng; Mary C. Scott 2026-09-25 16:55 Sodium expulsion from sodium closo-hydroborates under electron beam induced bias same sample

Materials Studied 2 materials

Material Family Role(s) Ion
Na2B10H10  · NBH10
Purchased precursor (not made for this work); listed in the SI of Deysher et al., Nat. Energy 2024, https://doi.org/10.1038/s41560-024-01569-9.
Purchased / commercial
Borohydride / complex hydride
Inorganic SE
 Electrolyte Na
Na4(B10H10)(B12H12)  · NBH
Made following an earlier paper https://doi.org/10.1038/s41560-024-01569-9
Borohydride / complex hydride
Inorganic SE
 Electrolyte Na

Declared for sample NBH-2024-12-CRYO — shared by every dataset on this sample.

Experiment Metadata

Spot Size 14.0
Image Size 3072x2048
Visibility public
Beam Current 6.4
Recorded Data TIFF image frames and .avi movies (frames combined into movie sequences)
Detector Mode ETD secondary electron (SE), high vacuum
Publication Doi 10.1093/mam/ozag104
Sample Transfer Inert (Ar) transfer from the glovebox using a Thermo Fisher Scientific (TFS) QuickConnect sample loader
Chamber Pressure 0.944
Source Folder(S) cryo SEM dose exp Mixed NBH/6.4nA exp1; cryo SEM dose exp Mixed NBH/6.4 exp 2; cryo SEM dose exp Mixed NBH/6.2 exp 3
Working Distance 8.25-8.26
Institution Code ESRA
Instrument Model Thermo Fisher Aquilos DualBeam (SEM/FIB), FEG source
Specimen Geometry top-down
Reference Still(S) cryo SEM dose exp Mixed NBH/6.4nA exp1/6.4nA exp1/pre 5kv to image 20kx 6.4nA_003.tif; cryo SEM dose exp Mixed NBH/6.4 exp 2/6.4 exp 2/10kx.tif; cryo SEM dose exp Mixed NBH/6.2 exp 3/6.2 exp 3/10kx_001.tif
Sample Temperature cryo
Sample Preparation Pelletized NBH powder prepared in an Ar glovebox; pellet fixed to the SEM stub with carbon tape
Detector Mode Source TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 6.4nA_003.tif
Data Location (Local) I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\6.4nA exp1; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\6.4 exp 2; I:\Data\NBH\SEM NBH Beam damage experiments\cryo SEM dose exp Mixed NBH\6.2 exp 3
Accelerating Voltage Kv 5.0
Instrument Model Source TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 6.4nA_003.tif
Stage Temperature (Header) 79.2
Dwell Time (Reference Still) 3.0
Experiment Folders In Record 3.0
Stage Tilt (Reference Still) 0.0
Accelerating Voltage Kv Source TIFF header (Thermo Fisher FEI metadata) of pre 5kv to image 20kx 6.4nA_003.tif
Acquisition Date(S) (Reference Stills) 2024-12-12
Horizontal Field Width (Reference Still) 20.7-41.4

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